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Beilstein J. Org. Chem. 2012, 8, 344–348, doi:10.3762/bjoc.8.38
Graphical Abstract
Scheme 1: Synthesis of 1-carbamoyl-2-oxopropyl acetates.
Scheme 2: Synthesis of 2,2-dihalo-N-phenylacetamides.
Scheme 3: Synthesis of dichloroacetamides. Reagents and conditions: 1 (1.0 mmol), dioxane (2 mL), DIB (1.3 eq...
Scheme 4: Synthesis of dibromoacetamides. Reagents and conditions: 1 (1.0 mmol), dioxane (2 mL), DIB (1.3 equ...
Scheme 5: Probe the mechanism.
Scheme 6: Tentative mechanism for the synthesis of 2,2-dihalo-N-phenylacetamides.
Beilstein J. Org. Chem. 2011, 7, 1436–1440, doi:10.3762/bjoc.7.167
Scheme 2: The synthesis of 1-carbamoyl-2-oxopropyl acetates. Conditions: 1 (1.0 mmol), DCE (2 mL), DIB (1.3 e...
Scheme 3: Possible reaction mechanism.